A Copper-polyol Complex: [Na2(C2H6O2)6][Cu(C2H4O2)2] - PubMed

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Abstract

The ionic title complex, bis(mu-ethylene glycol)-kappa(3)O,O':O';kappa(3)O:O,O'-bis[(ethylene glycol-kappa(2)O,O')(ethylene glycol-kappaO)sodium] bis(ethylene glycolato-kappa(2)O,O')copper(II), [Na(2)(C(2)H(6)O(2))(6)][Cu(C(2)H(4)O(2))(2)], was obtained from a basic solution of CuCl(2) in ethylene glycol and consists of discrete ions interconnected by O-H...O hydrogen bonds. This is the first example of a disodium-ethylene glycol complex cation cluster. The cation lies about an inversion center and the Cu(II) atom of the anion lies on another independent inversion center.

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Figures

Figure 1

Figure 1

The mol­ecular structure of (I),…

Figure 1

The mol­ecular structure of (I), showing the atom-numbering scheme. Displacement ellipsoids are drawn…

Figure 1 The mol­ecular structure of (I), showing the atom-numbering scheme. Displacement ellipsoids are drawn at the 40% probability level. Disordered atom O8B and methyl­ene H atoms have been omitted for clarity. [Symmetry codes: (i) formula image; (ii) formula image.]
Figure 2

Figure 2

A packing diagram of (I),…

Figure 2

A packing diagram of (I), viewed approximately down the a axis, showing the…

Figure 2 A packing diagram of (I), viewed approximately down the a axis, showing the hydrogen-bonding inter­actions between the anionic and cationic units. H atoms not involved in hydrogen bonding and disordered atom O8B have been omitted for clarity. [Symmetry codes: (ii) formula image; (iii) formula image; (v) formula image; (vi) formula image; (vii) formula image, formula image.]
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References

    1. Allen, F. H. (2002). Acta Cryst. B58, 380–388. - PubMed
    1. Altomare, A., Burla, M. C., Camalli, M., Cascarano, G. L., Giacovazzo, C., Guagliardi, A., Moliterni, A. G. G., Polidori, G. & Spagna, R. (1999). J. Appl. Cryst.32, 115–119.
    1. Antti, B.-M. (1976). Acta Chem. Scand. Ser. A, 30, 405–410.
    1. Antti, B.-M., Lundberg, B. K. S. & Ingri, N. (1972). Acta Chem. Scand. Ser. A, 26, 3984–3994.
    1. Bonet, F., Tekaia-Elhsissen, K. & Sarathy, K. V. (2000). Bull. Mater. Sci.23, 165–168.
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