Halogenide Von 3d‐Metallen: [V(NH3)6]I2, [Cr(NH3)6]I2, [Mn(NH3)6 ...

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  • DOI:10.1002/ZAAC.19966220709
  • Corpus ID: 96787877
Isotype Strukturen einiger Hexaamminmetall(II)‐halogenide von 3d‐Metallen: [V(NH3)6]I2, [Cr(NH3)6]I2, [Mn(NH3)6]Cl2, [Fe(NH3)6]Cl2, [Fe(NH3)6]Br2, [Co(NH3)6]Br2 und [Ni(NH3)6]Cl2@article{Essmann1996IsotypeSE, title={Isotype Strukturen einiger Hexaamminmetall(II)‐halogenide von 3d‐Metallen: [V(NH3)6]I2, [Cr(NH3)6]I2, [Mn(NH3)6]Cl2, [Fe(NH3)6]Cl2, [Fe(NH3)6]Br2, [Co(NH3)6]Br2 und [Ni(NH3)6]Cl2}, author={Ralf Essmann and Guido Kreiner and Anke Niemann and D. Rechenbach and Axel Schmieding and Th. Sichla and Uwe Zachwieja and Herbert Jacobs}, journal={Zeitschrift f{\"u}r anorganische und allgemeine Chemie}, year={1996}, volume={622}, pages={1161-1166}, url={https://api.semanticscholar.org/CorpusID:96787877} }
  • R. EssmannG. Kreiner+5 authors H. Jacobs
  • Published 1 July 1996
  • Chemistry
  • Zeitschrift für anorganische und allgemeine Chemie
Durch Umsetzungen von VI2 und CrI2 mit flussigem Ammoniak bei Raumtemperatur wurden gelbe Kristalle von [V(NH3)6]I2 bzw. grune von [Cr(NH3)6]I2 erhalten. Farbloses [Mn(NH3)6]Cl2 wurde durch Umsetzung von Mn mit NH4Cl in uberkritischem Ammoniak einkristallin dargestellt. Farblose und transparente Kristalle von [Fe(NH3)6]Cl2 und [Fe(NH3)6]Br2 konnten durch Umsetzung von FeCl2 bzw. FeBr2 in uberkritischem Ammoniak bei 400°C erhalten werden. Wird unter den gleichen Bedingungen Tri-μ-amido-bis… ExpandView via PublisherSave to LibrarySaveCreate AlertAlertCiteShare44 CitationsHighly Influential Citations1Background Citations1 Results Citations2View All

44 Citations

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Reactions of transition-metal cations with [Re6Te8(CN)6]4−: syntheses and structures of [Zn(NH3)4]2[Re6Te8(CN)6], [{Co(NH3)5}2Re6Te8(CN)6] · 4H2O, and [{Ni(NH3)5}2Re6Te8(CN)6] · 4H2O

    K. BrylevP. SekarN. NaumovV. FedorovJ. IbersChemistry
  • 2004
  • 12
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Homoleptic Octahedral Methylamine Complexes of Manganese(II): Solvothermal Syntheses and Crystal Structures of [Mn(NH2CH3)6]Cl2 and the Pentaselenide [Mn(NH2CH3)6]Se5

    O. KysliakJ. DanielsG. SchnakenburgJ. BeckChemistry
  • 2012
[Mn(NH2CH3)6]Cl2 (1) and [Mn(NH2CH3)6]Se5 (2) were prepared by solvothermal reactions in liquid methylamine from MnCl2 at 150 °C for 1 and from a mixture of MnCl2, Rb2Se and selenium at 120 °C for 2.… Expand
  • 10
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Chalcogenidotellurates(IV) (TeS3)2– and (TeSe3)2– by Low-Temperature Solvothermal Synthesis from Liquid Ammonia and Methylamine

    O. KysliakJ. BeckChemistry, Materials Science
  • 2013
The novel chalcogenidotellurates(IV) [Zn(NH3)6][Zn(NH3)4]2(TeS3)3 (1), [Zn(NH3)4](TeSe3) (2), [Mn(NH3)6](TeS3) (3), [Mn(NH3)6](TeSe3) (4) and [Mn(CH3NH2)6](TeSe3) (5) were obtained by solvothermal… Expand
  • 13
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Ammonia Uptake and Release in the MnX2–NH3 (X = Cl, Br) Systems and Structure of the Mn(NH3)nX2 (n = 6, 2) Ammines

    Hazel ReardonJames M. HanlonM. GrantImogen FullbrookD. GregoryChemistry
  • 2012
Hexa-ammine complexes, Mn(NH3)6X2 (X = Cl, Br), have been synthesized by ammoniation of the corresponding transition metal halide and characterized by Powder X-ray diffraction (PXRD) and Raman… Expand
  • 26
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Ammine-Stabilized Transition-Metal Borohydrides of Iron, Cobalt, and Chromium: Synthesis and Characterization.

    Elsa RoedernT. JensenChemistry, Materials ScienceInorganic chemistry
  • 2015
TLDRThe decomposition mechanisms of the prepared compounds along with the composites [Fe(NH3)6](BH4)2·nNH3BH3 (n = 2, 4, 6) were studied by thermal analysis and in situ SR-PXD, which allowed for the removal of inert metal halides.Expand
  • 32
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Synthesis, Crystal Structure, and IR Investigations of [(NH3)5V ? O ? V(NH3)5]I4 · NH3 and [(NH3)5Ti ? O ? Ti(NH3)5]I4 · NH3

    T. SichlaR. NiewaU. ZachwiejaH. JacobsR. EssmannChemistry
  • 1996
The reaction of VI2 or TiI3, respectively, with ammonia in the presence of traces of water or oxygen, respectively, leads to [(NH3)5MOM(NH3)5]I4 · NH3 with M = V, Ti. Their structures were solved by… Expand
  • 3
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Syntheses and Characterization of Diammine-Nickel/Cobalt(II)-Bisdicyanamide M(NH3)2[N(CN)2]2 with M = Ni and Co.

    Markus MannDamian MrozLaura HenrichA. HoubenJ. van LeusenR. DronskowskiChemistryInorganic chemistry
  • 2019
TLDRX-ray single-crystal structure analyses show that M(NH3)2[N(CN)2]2 with M = Ni and Co crystallize isotypically to each other and adopt the monoclinic space group P21/ c (no. 14), which shows that the dicyanamide moiety is a medium-field ligand.Expand
  • 3
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Chalcogenidoantimonates by Solvothermal Synthesis in Liquid Ammonia

    O. KysliakJ. BeckMaterials Science, Chemistry
  • 2013
A series of chalcogenidoantimonates, namely [Zn(NH3)6](SbIII4S7) (1), [Zn(NH3)6]{Zn(NH3)3SbVS4}2·NH3 (2), [Mn(NH3)6](SbIIISe2)2 (3) and [Zn(NH3)4]{Zn(NH3)SbIIISe3}2·3NH3 (4) are synthesized by… Expand
  • 5
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Preparation and Crystal Structures of Ni(NH3)2Cl2 and of Two Modifications of Ni(NH3)2Br2 and Ni(NH3)2I2

    A. LeineweberH. JacobsChemistry
  • 2000
Abstract Diammine nickel(II) halides, Ni(NH 3 ) 2 X 2 ( X =Cl, Br, I), were prepared by decomposition of the corresponding hexaammines at 120°C in dynamical vacuum. Their crystal structures are of… Expand
  • 14
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Synthesis, Structure and NH3 Sorption Properties of Mixed Mg1-xMnx(NH3)6Cl2 Ammines

    Perizat BerdiyevaA. Karabanova+4 authors S. DeleddaMaterials Science, ChemistryEnergies
  • 2020
This paper describes the synthesis, crystal structure, and NH3 sorption properties of Mg1-xMnx(NH3)6Cl2 (x = 0–1) mixed metal halide ammines, with reversible NH3 storage capacity in the temperature… Expand
  • 4
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11 References

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Hydrogen bonding in hexamminenickel(II) salts [Ni(NH3)6]X2(X− = Cl−, Br−, I−, NO−2, NO−3, BF−4, ClO−4) — acceptor strength of anions

    R. EssmannChemistry
  • 1995
  • 17
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Hydrogen bonding in hexamminemetal(II) bromides [M(NH3)6]Br2 (M2+ = Ca2+, Mn2+, Fe2+, Co2+, Ni2+, Cu2+, Cd2+) — synergetic effect of M2+

    R. EssmannChemistry
  • 1995
  • 14
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Hochdrucksynthese der η-phase im System Mn-N: Mn3N2

    H. JacobsC. StüveChemistry
  • 1984
  • 53
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Einkristallzüchtung von γ′-Fe4N in überkritischem ammoniak

    H. JacobsJ. BockMaterials Science
  • 1987
  • 25
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Röntgenographische Strukturbestimmung und IR-spektroskopische Untersuchungen an Hexaammindiiodiden, [M(NH3)6]I2, von Eisen und Mangan

    H. JacobsJ. BockC. StüveChemistry
  • 1987
  • 20
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Revised effective ionic radii and systematic studies of interatomic distances in halides and chalcogenides

    R. D. ShannonChemistry
  • 1976
The effective ionic radii of Shannon & Prewitt [Acta Cryst. (1969), B25, 925-945] are revised to include more unusual oxidation states and coordinations. Revisions are based on new structural data,… Expand
  • 50,425
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The Magnetic Investigation of Mn ++ , Co ++ , Ni ++ and Cu ++ Ammine and Anhydrate Salts at Low Temperatures

    Takashi WatanabePhysics
  • 1961
The magnetic susceptibility measurements of ammine salts and an-hydrate salts of Mn ++ , Co ++ , Ni ++ and Cu ++ ions at the temperature above 90°K have been carried out previously by Kido and the… Expand
  • 11
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Magnetochemische Untersuchungen. VIII. Die Konstitution. Einiger einfacher Kobalt‐ und Nickelverbindungen, beurteilt auf Grund ihres magnetischen Verhaltens

    W. KlemmW. SchüthChemistry
  • 1933
Es wird der Bindungszustand der Oxyde, Sulfide und Halogenide des Nickels und Kobalts auf Grund ihres magnetischen Verhaltens beurteilt. NiO und CoO sind als Ubergangsglieder von den para- zu den… Expand
  • 16
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Diffractometer devices controlled by a personal computer

    J. LangeH. BurzlaffComputer Science
  • 1991
TLDRThe application of single-board microcomputers as programmable interfaces simplifies the construction of complex diffractometer control units and unburden the personal computer and simplify the development of the diffractometers measuring program.Expand
  • 11
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Computing in crystallography

    R. DiamondS. RamaseshanK. VenkatesanComputer Science, Materials Science
  • 1980
  • 135
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