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  • DOI:10.1021/ACS.CHEMMATER.5B00411
  • Corpus ID: 73595106
Structural Investigation of Graphitic Carbon Nitride via XRD and Neutron Diffraction@article{Fina2015StructuralIO, title={Structural Investigation of Graphitic Carbon Nitride via XRD and Neutron Diffraction}, author={Federica Fina and Samantha K. Callear and George M. Carins and John T. S. Irvine}, journal={Chemistry of Materials}, year={2015}, volume={27}, pages={2612-2618}, url={https://api.semanticscholar.org/CorpusID:73595106} }
  • Federica FinaS. Callear+1 author J. Irvine
  • Published 2 April 2015
  • Materials Science, Chemistry
  • Chemistry of Materials
Graphitic carbon nitride (g-C3N4) has, since 2009, attracted great attention for its activity as a visible-light-active photocatalyst for hydrogen evolution. Since it was synthesized in 1834, g-C3N4 has been extensively studied both catalytically and structurally. Although its 2D structure seems to have been solved, its 3D crystal structure has not yet been confirmed. This study attempts to solve the 3D structure of graphitic carbon nitride by means of X-ray diffraction and of neutron… ExpandView via Publisherresearch-repository.st-andrews.ac.ukSave to LibrarySaveCreate AlertAlertCiteShare706 CitationsHighly Influential Citations25Background Citations35 Methods Citations5 Results Citations3View All

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706 Citations

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Local Structural Analysis of Graphitic Carbon Nitrides

    Diane M HaiberM. TreacyP. CrozierMaterials Science, ChemistryMicroscopy and Microanalysis
  • 2018
Graphitic carbon nitrides are layered, polymeric compounds that are widely studied as a semiconducting support for visible-light driven photocatalytic water splitting [1]. However, structural… Expand
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Determination of Crystal Structure of Graphitic Carbon Nitride: Ab Initio Evolutionary Search and Experimental Validation

    Junjie WangDong HaoJinhua YeN. UmezawaMaterials Science, Chemistry
  • 2017
Although graphitic carbon nitride (g-C3N4) is a promising photofunctional material, its structure is poorly understood. Here, we present a systematic study of stable crystal structures of g-C3N4 by… Expand
  • 93
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Structural and optical properties of carbon nitride polymorphs

    L. StagiD. ChiriuC. M. CarbonaroR. CorpinoP. RicciMaterials Science, Chemistry
  • 2016
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Synthesis of graphitic carbon nitride under low ammonia partial pressure

    Hiroya InokiG. SeoK. KanaiChemistry, Materials Science
  • 2020
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Facile hydrothermal preparation of graphitic carbon nitride supercell structures with enhanced photodegradation activity

    Ge XuYanheng XuZhicun ZhouYiwen BaiMaterials Science, Environmental ScienceDiamond and Related Materials
  • 2019
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Elucidating the structure of the graphitic carbon nitride nanomaterials via X-ray photoelectron spectroscopy and X-ray powder diffraction techniques.

    E. AlwinW. NowickiR. WojcieszakM. ZielińskiM. PietrowskiMaterials Science, ChemistryDalton transactions
  • 2020
TLDRIt is allowed to state that the carbon nitride structure prepared by the thermal condensation of dicyandiamide is closer to the structure in which poly(aminoimino)heptazine subunits are linked into chains rather than the structure involving fully-condensed poly heptazine network.Expand
  • 69
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A comparative study on modified graphitic carbon nitride: Synthesis, characterization, and applications

    Z. SyrgiannisK. ChristoforidisMaterials ScienceHandbook of Carbon-Based Nanomaterials
  • 2021
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Nickel doped graphitic carbon nitride nanosheets and its application for dye degradation by chemical catalysis

    D. DasD. Banerjee+5 authors K. ChattopadhyayChemistry, Materials Science
  • 2018
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Synthesis of Graphitic Carbon Nitride on the Surface of Fe3O4 Nanoparticles

    E. B. ChubenkoA. V. BaglovYu. A. FedotovaV. BorisenkoMaterials Science, ChemistryInorganic Materials
  • 2021
A composite material consisting of graphitic carbon nitride and iron(II,III) oxide (g-C3N4/Fe3O4) and having photocatalytic and magnetic properties has been synthesized via single-step thermal… Expand
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Templated Synthesis of Exfoliated Porous Carbon with Dominant Graphitic Nitrogen

    Esmail DoustkhahA. Kotb+4 authors M. H. N. AssadiMaterials Science, ChemistryACS materials Au
  • 2023
We present here a new approach for the synthesis of nitrogen-doped porous graphitic carbon (g-NC) with a stoichiometry of C6.3H3.6N1.0O1.2, using layered silicate as a hard sacrificial template.… Expand
  • 12
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23 References

Citation TypeHas PDFAuthorMore FiltersMore FiltersFiltersSort by RelevanceSort by Most Influenced PapersSort by Citation CountSort by Recency

Graphitic carbon nitride materials: variation of structure and morphology and their use as metal-free catalysts

    Arne ThomasA. Fischer+4 authors J. CarlssonMaterials Science, Chemistry
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Graphitic carbon nitride, g-C3N4, can be made by polymerization of cyanamide, dicyandiamide or melamine. Depending on reaction conditions, different materials with different degrees of condensation,… Expand
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On the validity of the formation of crystalline carbon nitrides, C3N4

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Polymeric graphitic carbon nitride as a heterogeneous organocatalyst: from photochemistry to multipurpose catalysis to sustainable chemistry.

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Polymeric graphitic carbon nitride materials (for simplicity: g-C(3)N(4)) have attracted much attention in recent years because of their similarity to graphene. They are composed of C, N, and some… Expand
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Synthesis of Nitrogen-Rich Carbon Nitride Networks from an Energetic Molecular Azide Precursor

    E. G. GillanMaterials Science, Chemistry
  • 2000
Nitrogen-rich carbon nitrides are produced as amorphous, bulk solids from the slow thermal decomposition of 2,4,6-triazido-1,3,5-triazine [(C3N3)(N3)3]. This energetic molecular azide is thermally… Expand
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Novel group 14 nitrides

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Crystal structure of polymeric carbon nitride and the determination of its process-temperature-induced modifications

    T. TyborskiC. MerschjannS. OrthmannF. YangM. Lux-SteinerT. Schedel-NiedrigMaterials ScienceJournal of physics. Condensed matter : an…
  • 2013
TLDRIt is found that both triazine- and heptazine-based g-C3N4 can only account for minor phases within the investigated synthesis products.Expand
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Thermal Conversion of Guanylurea Dicyanamide into Graphitic Carbon Nitride via Prototype CNx Precursors

    B. LotschW. SchnickChemistry, Materials Science
  • 2005
Guanylurea dicyanamide, [(H2N)C(O)NHC(NH2)2][N(C⋮N)2], has been synthesized by ion exchange reaction in aqueous solution and structurally characterized by single-crystal X-ray diffraction (C2/c, a =… Expand
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Unmasking melon by a complementary approach employing electron diffraction, solid-state NMR spectroscopy, and theoretical calculations-structural characterization of a carbon nitride polymer.

    B. LotschM. Döblinger+4 authors W. SchnickMaterials Science, ChemistryChemistry
  • 2007
TLDRThe polymeric character and thermal stability of melon might render this polymer a pre-stage of g-C(3)N(4) and portend its use as a promising inert material for a variety of applications in materials and surface science.Expand
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Photodegradation performance of g-C3N4 fabricated by directly heating melamine.

    Shi YanZhaosheng LiZ. ZouChemistry, Environmental ScienceLangmuir : the ACS journal of surfaces and…
  • 2009
TLDRThe results clearly indicate that the metal-free g-C(3)N(4) has good performance in photodegradation of organic pollutant.Expand
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Melem (2,5,8-triamino-tri-s-triazine), an important intermediate during condensation of melamine rings to graphitic carbon nitride: synthesis, structure determination by X-ray powder diffractometry, solid-state NMR, and theoretical studies.

    B. JürgensE. IrranJ. SenkerP. KrollH. MüllerW. SchnickMaterials Science, ChemistryJournal of the American Chemical Society
  • 2003
TLDRA good agreement was found between the observed and calculated structural parameters and also for the vibrational frequencies of melem according to temperature-dependent X-ray powder diffractometry investigations above 560 degrees C, melem transforms into a graphite-like C-N material.Expand
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