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  • DOI:10.1021/IC960974L
  • Corpus ID: 93230270
Synthesis and X-ray Structure of the Mononuclear Nine-Coordinate Gadolinium(III) Hydrogen Oxydiacetate [Gd(C4H5O5)3]·C4H6O5·H2O@article{Baggio1997SynthesisAX, title={Synthesis and X-ray Structure of the Mononuclear Nine-Coordinate Gadolinium(III) Hydrogen Oxydiacetate [Gd(C4H5O5)3]·C4H6O5·H2O}, author={Ricardo F. Baggio and Mar{\'i}a Teresa Garland and Mireille Perec}, journal={Inorganic Chemistry}, year={1997}, volume={36}, pages={950-952}, url={https://api.semanticscholar.org/CorpusID:93230270} }
  • R. BaggioM. GarlandM. Perec
  • Published 26 February 1997
  • Chemistry
  • Inorganic Chemistry
A new mononuclear gadolinium(III) complex [Gd(Hoda)3]·H2oda·H2O (Hoda = HO2CCH2OCH2CO2-) has been isolated from the reaction of Gd2O3 with oxydiacetic acid in aqueous solution. A single-crystal X-ray study features the nine-coordinate GdO9 core in a distorted tricapped trigonal-prism environment. The top and bottom triangles are defined by three carboxylate and three carbonyl oxygen atoms, respectively, and the capping positions, by three ether oxygens of three tridentate Hoda ligands. View via PublisherSave to LibrarySaveCreate AlertAlertCiteShare17 CitationsView All

17 Citations

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Synthesis and structure of two polymeric barium–oxydiacetates: [Ba(oda) · H2O]n and [Ba(Hoda)2]n (H2oda: oxydiacetic acid)

    R. BaggioM. GarlandG. LeyvaM. PerecG. PollaMaterials Science, Chemistry
  • 2004
  • 13
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Synthesis and X-ray crystal determination of four novel lanthanide (III) oxydiacetate complexes

    R. BaggioM. GarlandM. PerecChemistry
  • 1998
  • 21
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Novel europium and gadolinium compounds in the lanthanide(III) oxydiacetate series

    P. AramendíaR. BaggioM. GarlandM. PerecChemistry, Materials Science
  • 2000
  • 21
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Crystal structures and luminescent properties of terbium(III) carboxylates

    B. BarjaR. BaggioM. GarlandP. AramendíaO. PeñaM. PerecChemistry, Materials Science
  • 2003
  • 71
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Synthesis and molecular structure of oxydiacetate complexes of nickel(II) and cobalt(II). Theoretical analysis of the planar and non-planar conformations of oxydiacetate ligand and oxydiacetic acid

    A. GrirraneAntonio PastorA. IencoC. MealliAgustín GalindoChemistry
  • 2002
A novel synthetic route to [Ni(oda)(H2O)3]·1.5H2O 1 and [Co(oda)(H2O)2]·H2O 2 [oda = oxydiacetate, O(CH2CO2−)2] is presented. These complexes react with bidentate N-donor ligands to yield compounds… Expand
  • 41
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A novel nonacoordinate bridging selenido ligand in a tricapped trigonal- prismatic geometry. X-Ray structure of Cu11(μ9-Se)(μ3-Br)3[Se2P(OPri)2]6

    C. W. LiuChiu-Mine HungHsiu-Chih ChenJu‐Chung WangTai-Chiun KengK. GuoChemistry
  • 2000
The first nonacoordinate bridging selenido ligand in a tricapped trigonal prismatic geometry, Cu11(μ9-Se)(μ3-Br)3[Se 2P(OPri)2]6, is prepared along with closed-shell ion-centered CuI8 cubes, … Expand
  • 23
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Mixed 3d/4f polynuclear complexes with 2,2′-oxydiacetate as bridging ligand: Synthesis, structure and chemical speciation of La–M compounds (M=bivalent cation)

    S. DomínguezJ. Torres+4 authors C. KremerChemistry
  • 2007
  • 18
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Lanthanide complexes with oda, ida, and nta: From discrete coordination compounds to supramolecular assemblies

    C. KremerJ. TorresS. DomínguezChemistry
  • 2008
  • 52
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Synthesis and structural characterization of lanthanide oxalate–oxydiacetate mixed-ligand coordination polymers {[Ln(oda)(H2O) x ]2(ox)} n ( x = 3 for Ln = La, Ce, Pr, Gd, Tb and x = 2 for Ln = Er)

    Yong-hong WenXiao-Hui WuSai BiShusheng ZhangChemistry, Materials Science
  • 2009
Reactions of oxydiacetic acid (H2oda) with lanthanide oxide, nitrate, chloride, and carbonate gave six lanthanide oxalate–oxydiacetate mixed-ligand coordination polymers {[Ln(oda)(H2O) x ]2(ox)} n [x… Expand
  • 12
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Syntheses, crystal structures, and some properties of heavier lanthanide(III) complexes with optically active N,N ′-bis(2-hydroxybenzyl)-N,N ′-bis(2-pyridylmethyl)-R-1,2-propanediamine

    Y. YamadaShinobu TakenouchiYusuke MiyoshiK. OkamotoChemistry
  • 2010
The reaction of N,N′-bis(2-hydroxybenzyl)-N,N′-bis(2-pyridylmethyl)-R-1,2-propanediamine (R-bbppnH2) with Ln(NO3)3 · nH2O (Ln = Tb, Dy, Ho, Er, Tm, Yb, or Lu) stereoselectively gave an optically… Expand
  • 9
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